Barium Titanate and Wax Capacitor - K=12.5 to 18.6 (Sept. 9, 2004)

This was a flat plate capacitor consisting of barium titanate (BaTiO3) and paraffin wax. It was made at a Weird Science weekend with friends on September 4, 2004. The K was measured using two different instruments as either 12.5 or 18.6.

Making the barium titanate and wax dielectric

The paraffin wax was melted indoors in a can on the stove and then brought outdoors and placed on my digital scale for measuring the ingredients. The barium titanate was then mixed in with the wax. From the measurements with the scale the mix was 44% barium titanate and 66% paraffin wax by weight.

The setup for making the barium titanate and wax dielectic.
The barium titanate and wax mix in a can.

A box mold was made using aluminium flashing and aluminium tape (both available in hardware stores.) The mix was then scooped up from the can and placed into the mold. The result was a nice thick paste which hardened quickly as the wax cooled.

The aluminium flashing mold before pouring in the barium
      titanate and wax mix.
The barium titanate and wax mix in the mold.

Measuring the dielectric constant of the barium titanate and wax dielectric

The dielectric constant is the ratio of the capacitance of the capacitor with the dielectric being tested to the capacitance of the same capacitor but with air as the dielectric.

To measure the capacitance with the dielectric, a solid round metal plate was placed on a jar, followed by the dielectric material, followed by a round piece of aluminium foil (see left photo below.) Then, to compress the foil plate a piece of foam with four access holes was placed on the foil (see right photo below.)

The finished barium titanate and wax dielectric sitting between
      electrodes in preparation for measuing the capacitance.
A piece of form material sitting on the top electrode.

Weight was then placed on the foam to firmly press the whole thing together (see photo below.) Two different meters were available to make independent measurements of the capacitance.

Weight added to the top of the whole thing.

Measurements were then made using the four access holes in the foam and an average was taken (see left photo below.) Note that this includes the capacitance of the meter probes and the meter itself. This had to be eliminated so an additional measurement was taken with the meter probes spaced apart by the thickness of the dielectric but with air between them (see right photo below.) This was to measure the capacitance of the meter without the dielectric. This value was then subtracted from the previously obtained average capacitance with the dieletric to get the value for the capacitor with dielectric alone. For the two meters, the values were 134pF and 199pF.

Measuring the capacitance of the barium titanate and wax
      dielectric.
Checking the capacitance with the meter probes separated by 
      the same distance.

Next, the capacitance of the capacitor with just air as the dielectric was needed. Rather than measuring this, it was calculated using the normal formula for a plate capacitor giving 10.7pF. The dielectric constant with the two different capacitors were therefore:
K1 = 134pF / 10.7pF = 12.5
K2 = 199pF / 10.7pF = 18.6
Both these were pretty respectable values given that most insulators are in the 2 to 3 range.

Measuring the resistance of the barium titanate and wax dielectric

Just in case, we also measured resistance of the barium titanate powder with the meter probes spaced about 2cm apart and got 4Mohms. We then made a similiar measurement with the dielectric and got 2.31Mohms. This was too low for our purposes. Given that the high voltage power supply we were going to test with could supply 80kV, we calculated the current that would go through the dielectric as 34.6mA (80kV/2.31Mohms). We then measured the resistance of 1/16" thick paraffin wax and got > 20Mohms.

Figuring that moisture might be the issue, we put the dielectric in the oven at 110C (230F) for 65 minutes and measured resistance again. The resistance of the dielectric was now > 20Mohms, so moisture was likely the problem.

Propulsion testing of the barium titanate and wax dielectric

Applying a range of high voltages with the capacitor on a digital scale, it showed no sign of weight change.

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